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Abstracts of Awards for FY1999
Small Business Innovation Research for FY1999 (SBIR)
Department of Commerce Program Solicitation

Introduction

The Department of Commerce (DOC), through the Small Business Innovation Research (SBIR) program, awarded 27 Phase 1 contracts for FY 1999. These awards of up to $75,000 each, and totaling approximately $2.9 million, are for a 6-month effort to demonstrate the feasibility of innovative approaches to the research topics identified in the "DOC SBIR Program Solicitation for FY99 (DOC 99-1)." Abstracts of the successful Phase 1 proposals submitted under this solicitation, and brief comments on their potential commercial applications, are provided in this publication. In Phase 2, funding is provided for projects that are most promising after Phase 1 is completed. These awards can be for up to $300,000 each and for 2 years. Phase 3 uses non-SBIR funding to pursue potential commercial applications of the project. The DOC awarded a total of 10 Phase 2 contracts in FY 99 for a total of approximately $4.6 million. Abstracts of successful Phase 2 proposals and comments on their commercial applications are also provided in this solicitation.

The SBIR program is highly competitive. A total of about 300 proposals were received by DOC in response to its FY 99 solicitation. The proposals were independently reviewed by DOC scientists and/or engineers. With the funds available, only 40 could be selected. Final selection was based upon the results of the reviews, relative importance to DOC needs, relationship to on-going research, and potential for commercialization.

Go to the NIST SBIR Awards by State.

Note: Certain non-ASCII characters may not be represented accurately in this document. In cases where there may be doubt, please refer to the printed copy of the solicitation or direct your questions to sbir@nist.gov.

FY1999 Phase 1 Award Winner

TOPIC: 8.6. Adaptive Learning Systems

SUBTOPIC: 8.6.1T Web-based Instructional Platforms

TITLE: Adaptive Learning in Web-Based Instructional Systems

NIST OU: 890

FIRM: Intelligent Systems Technology, Inc.

2800 28th Street, Suite 306

Santa Monica, CA 90405

PRINCIPAL INVESTIGATOR: Azad Madni

310-581-5440

AWARD AMOUNT: $74,891

ABSTRACT:

Recent advances in information technologies, and more specifically, in web-based instruction, intelligent tutoring systems, and platform-independent implementations have made it possible for the first time to create web-based instructional systems with the capability to adapt instructional sequence, and presentations based on learner/student progress and entry level skills. The specific thrust of this SBIR is intelligent authoring and knowledge management in web-based instructional systems. The product of Phase 1 will be a conceptual prototype that communicates the Phase 2 functionality and features to end-users and sponsors for feedback and critique.

COMMERCIAL APPLICATIONS:

Potential commercial applications of the research include web-based distance learning/training for packaged application suites such as ERP systems, manufacturing execution systems, and decision support systems.

FY1999 Phase 1 Award Winner

TOPIC: 8.7 Advanced Building Materials and Systems

SUBTOPIC: 8.7.5T Measurement of Thermal Conductivity of Insulation at High Temperature

TITLE: High Temperature Thermal Conductivity Apparatus

NIST OU: 860

FIRM: MetSys Corporation

P.O. Box 317

Millwood, VA 22646

PRINCIPAL INVESTIGATOR: Daniel Flynn

540-837-2186

AWARD AMOUNT: $75,000

ABSTRACT:

It is proposed to develop an advanced-design guarded hot plate apparatus that will define the new state of the art for measuring the thermal conductivity of industrial insulation materials over the range of temperatures from 200 to 1500 K, depending upon the particular material and its compatibility with other materials. The apparatus will have the capability to carry out measurements under controlled environments of air, selected gases, or vacuum, again depending upon material compatibility. The specific technical objectives of the Phase 1 development effort are to: develop performance criteria and specifications for the apparatus; review alternative measurement approaches, select the design, and refine it to the point where it can be subjected to detailed analysis; develop numerical and analytical models of the apparatus that will enable reliable prediction of apparatus performance and measurement accuracy as functions of the design parameters; study and analyze alternative approaches to the most crucial design features of the apparatus; and develop a detailed design of the complete prototype apparatus to be built in Phase 2, and all instrumentation and software specifications.

COMMERCIAL APPLICATIONS:

Industrial plants and utilities account for about half of the total United States energy use. It has been estimated that over 1.4 quadrillion Btu's could be saved if industry installed economically optimal insulation. The apparatus to be developed under this project will provide the U.S. with an unparalled capability to provide accurate thermal conductivity data to manufacturers and users of high-temperature thermal insulations for a wide variety of industrial and military applications, thus allowing selection and installation of greatly improved insulation systems.

FY1999 Phase 1 Award Winner

TOPIC: 8.8 Advanced Detection and Suppression of Fires

SUBTOPIC: 8.8.1T Advanced Detection and Monitoring of Fires

TITLE: Novel Fiber Networked Diode Laser-Based Fire Detection

NIST OU: 860

FIRM: Physical Sciences, Inc.

20 New England Business Center

Andover, MA 01810-1077

PRINCIPAL INVESTIGATOR: William Kessler

978-689-0003

AWARD AMOUNT: $74,985

ABSTRACT:

Physical Sciences Inc. proposes to develop and demonstrate a fiber optic network of sensors for the detection of molecular species and smoke used as fire indicators. The combination of these two sensors in one package will preclude false alarms while providing rapid, sensitive fire detection. The all-fiber network will use absorption measurements for toxic gases and scattering measurements for the presence of smoke. Diode laser-based absorption spectroscopy utilizing near infrared light sources has been developed and refined now for more than 10 years. We propose advancing this technology to the next logical stop by integrating a diode laser-based carbon monoxide sensor and scattering smoke sensor with an all-fiber-optic network for transmission of the laser light to and from the measurement point. The use of the same fiber optic components for laser launch and reception reduces the cost of diode laser-based fire sensors for widespread commercial application. We envision a central hub location for the main sensor control networked to an array of sensors which may be located within an individual building, an industrial park, or an entire community.

COMMERCIAL APPLICATIONS:

We anticipate that the demonstrated fiber optic network of sensors may lay the foundation for a new class of fire sensors which provide fire and toxic gas detection capability for both the business community and communities of homeowners. The use of currently developed telecommunications products and new products about to come on-line in the telecommunications industry make it possible to envision fire and carbon monoxide sensor companies servicing businesses and individual homeowners in the coming years.

FY1999 Phase 1 Award Winner

TOPIC: 8.10 Condition-Based Maintenance

SUBTOPIC: 8.10.1T Development & Integration of Condition-Based Maintenance Technologies

TITLE: Vigilant: A Conditional-Based Maintenance Technology for

Turbomachines

NIST OU: 470

FIRM: The Athena Group, Inc.

3424 N.W. 31st Street

Gainsville, FL 32605

PRINCIPAL INVESTIGATOR: Iztok Koren

352-371-2567

AWARD AMOUNT: $75,000

ABSTRACT:

Condition-based maintenance (CBM) is concerned with ensuring the health of high-value systems. CBM is an evolving maintenance paradigm anticipated to play a major role in defining the operational environment of future complex machines. Such machines will be expected to possess deeply embedded diagnostic systems having predictably accurate real-time performance. A system with these capabilities would decrease operational costs and increase public safety. In this context, the Athena Group proposes Vigilant, a new class of embedded CBM system. The Vigilant paradigm is based on the innovative use of wavelets, neural classifiers, and data fusion techniques. By using multiple wavelet bases, the unresponsiveness of Fourier or single wavelet basis systems can be mitigated. Vigilant also incorporates a new data fusion and classifier design that overcomes the historical problem of training systems in the absence of meaningful failure databases. Preliminary studies have demonstrated the potential advantage of the Vigilant CBM in turbomachine applications. The Phase 1 SBIR study builds upon this foundation to produce an experimental prototype system that can be studied using computer simulations. The result is the definition of a viable Vigilant system which can be reduced to a field-operable prototype in Phase 2, and a commercial product in Phase 3.

COMMERCIAL APPLICATIONS:

CBM, while being an accepted maintenance paradigm, has had only limited commercial success. Vigilant expects to achieve a marketplace success in this area due to the technology's superior performance and cost-effectiveness. In commercial form, Vigilant will be delivered as a software system or upgrade. The marketing of Vigilant will benefit from the proposer's long-term technology relationship with Lockheed-Martin, a major provider of large complex machines.

FY1999 Phase 1 Award Winner

TOPIC: 8.11 Intelligent Control

SUBTOPIC: 8.11.3T Graphical Design of Manufacturing Control Systems

TITLE: Architectural Patterns for Real-Time Systems

NIST OU: 820

FIRM: Real-Time Innovations, Inc.

155A Moffett Park Drive, Suite 111

Sunnyvale, CA 94089

PRINCIPAL INVESTIGATOR: Rajive Joshi

408-720-8312

AWARD AMOUNT: $75,000

ABSTRACT:

Software architecture is critical for real-time systems. Much progress has been made in generic architectures and reference models; the NIST ISAM system presents a well-developed theory of temporal hierarchical modeling to structure real-time systems. However, generic architectures have not realized their potential for widespread adoption.

We believe this is largely due to a lack of enabling software tools. We propose to develop a capability to define and enforce architectural patterns, and merge it with a commercial software design environment for intelligent control. The tool will assist in defining the architecture, building compliant systems, and developing and reusing software modules. Architects will use patterns to specify generic system structures. Users will then create complex systems by filling in these templates. The tool will provide the much-needed mechanism for widespread use of reference architectures.

COMMERCIAL APPLICATIONS:

The proposed research will create a platform that will serve as a technology conduit for architectures, modules, and research. With a powerful development environment behind it, reference model architectures will realize the potential of long years of research. This research, if successful, will revolutionize the development of intelligent control systems.

FY1999 Phase 1 Award Winner

TOPIC: 8.11 Intelligent Control

SUBTOPIC: 8.11.5T Novel Atomizer for Control of Reference Spray Combustion Facility

TITLE: A Micromachined Device for Precision Atomization

NIST OU: 830

FIRM: Creare Incorporated

P.O. Box 71

Hanover, NH 03755

PRINCIPAL INVESTIGATOR: James J. Barry

603-643-3800

AWARD AMOUNT: $74,755

ABSTRACT:

To assist NIST's development of a reference spray combustion facility, we propose a novel atomizer based on a micromachined droplet generation device. This atomizer will provide precise and repeatable droplet fields, and its unique design permits control of droplet size distribution and spray output independent of air flow. We have previously demonstrated in the laboratory the basic approach for generating near-monodisperse droplets for production of precision aerosols. In Phase 1, we will demonstrate the generation of a specified droplet distribution using a proof-of-principle benchtop device and develop a concept design for a Phase 2prototype. Phase 2 will involve constructing the prototype device, testing it in the lab, then installing and testing the atomizer in the NIST combustion facility.

COMMERCIAL APPLICATIONS:

The end result of Phase 1 and 2 will be a precision atomizer ideally suited to the needs of NIST's reference facility. The technology has strong prospects for commercialization in combustion and in material processing applications requiring precise, well-controlled droplet distributions.

FY1999 Phase 1 Award Winner

TOPIC: 8.11 Intelligent Control

SUBTOPIC: 8.11.7T Process Monitoring and Control of Composites Processing

TITLE: Optical Coherence Tomography Based Fiber Optic Sensor for Monitoring and Control of Composites Processing

NIST OU: 850

FIRM: Optiphase Inc.

7652 Haskell Avenue

Van Nuys, CA 91406

PRINCIPAL INVESTIGATOR: Pepe Davis

925-876-8818

AWARD AMOUNT: $74,132

ABSTRACT:

An optical coherence tomography (OCT) based fiber optic sensor can provide non-invasive, high resolution, monitoring for control of composites processing in commercial manufacturing. OCT is a non-contact optical technique for imaging in scattering media such as glass reinforced composites. With <30 micron resolution achieved by OCT, microstructure and effects such as: fiber wetting, void structure, fiber orientation, fiber waviness, cracks and delaminations of composites can be determined. To commercialize this technology, a compact, robust, portable, and inexpensive OCT system must be designed and built which is insensitive to birefringence artifacts observed in typical OCT systems. Optiphase Inc. proposes to develop an innovative, all fiber optic OCT system utilizing a unique piezoelectric fiber optic modulator and a polarization sensitive design. Polarization sensitivity eliminates birefringence shadowing and artifacts and provides material strain information. The all fiber optic design provides compactness, ruggedness, portability and cost savings over bulk optic or hybrid systems. The project objectives are to design, build, and test this all fiber optic OCT sensor. These objectives will be met through analytical design and prototype testing culminating with imaging of glass reinforced composite samples at Lawrence Livermore National Laboratory.

COMMERCIAL APPLICATIONS:

The ruggedness, compactness, low cost, and non-invasive nature of an all fiber optic OCT system make this sensor applicable to monitoring, control, and automation of manufacturing processes and health monitoring of composites. In particular, an all fiber optic OCT sensor will be instrumental in monitoring microstructures during mold filling, predicting permeability for modeling of Liquid Composite Molding (LCM), and detecting damage such as cracks and delaminations of parts in the field. All these applications are specially pertinent to the automotive and marine composite industries. Additional commercial applications exist in the medical fields as a diagnostic tool for imaging of biological tissue such as the human retina, skin, blood vessels, and tooth and gums.

FY1999 Phase 1 Award Winner

TOPIC: 8.11 Intelligent Control

SUBTOPIC: 8.11.9T Sensor for In-Situ Measurements of Thermal Spray Coatings

TITLE: Investigation of Ripple-Technique for Thermal Spray Coatings

NIST OU: 850

FIRM: STRATONICS, Inc.

23151 Verdugo Drive, Suite 114

Laguna Hills, CA 92653

PRINCIPAL INVESTIGATOR: James Craig

949-461-7060

AWARD AMOUNT: $74,999

ABSTRACT:

Thermal spray coating (TSC) is a promising low-cost technology for improving the abrasion resistance and surface characteristics of low cost parts. The major problem preventing wider adoption of this technology, is that coating quality is very sensitive to the surface temperature of the substrate during deposition. Application of the ripple technique for the simultaneous measurement of sample emissivity and temperature to TSC will be investigated. All major sources of error will be identified. Experiments will be designed and carried out to quantify the magnitude of the possible errors. Special fixtures will be designed and constructed for these experiments. It is expected that a major source of error will be associated with the necessity to measure the TSC deposition-sample temperature through the TSC flame. Measurements will be made during operation of the TSC flame both with and without typical TSC deposition samples as a function of flame temperature, velocity, particle leading, and sample temperature, when applicable, to quantify this source of error. A second source of error is the failure to satisfy Kirchhoff's law with the ripple-technique lamps. Measurements will be carried out as a function of ripple-technique lamp location to quantify these errors.

COMMERCIAL APPLICATIONS:

The proposed ripple technique temperature measurement system addresses industry's needs to simultaneously measure emissivity and temperature in thermal spray coating processes. This product is well suited for researchers in national laboratories, universities and industries who are developing and improving TSC. Successful completion of the proposed Phase 1 and Phase 2 research will increase the market for optical-fiber thermometers and the associated instrumentation that supports the ripple technique. Currently, this market is confined to the application of the ripple technique to rapid thermal processing (RTP) of integrated circuit wafers.

FY1999 Phase 1 Award Winner

TOPIC: 8.11 Intelligent Control

SUBTOPIC: 8.11.10T High-Speed Video Camera for Measurements in Spray Processing

TITLE: Intelligent Control

NIST OU: 850

FIRM: The Cooke Corporation

600 Main Street, P.O. Box 888

Tonawanda, NY 14150-0888

PRINCIPAL INVESTIGATOR: Gerald Lilly

248-332-5655

AWARD AMOUNT: $65,000

ABSTRACT:

A need has been identified for a High Speed Video camera for the study of high velocity particles used in thermal spray applications. Cooke Corporation proposes to build on our past success in the area of high speed imaging of thermal sprays, by extending the capabilities of our video camera system. The proposed camera will have extended spectral range to allow imaging of sprays below 600C, while shortening exposure times to less than 50ns to enable the study of higher velocity sprays than previous systems. The camera will also provide multiple exposures per frame, with readout rates of 30 fps or lower as required. Spatial resolution of 10m or less will enable the imaging of fine droplets. All system parameters will be software controlled. The system will be robust, to allow operation in industrial environments. Deployment of the proposed high speed imaging system will further the research necessary to advance the industrial applications of spray forming in the industrial, military and automotive sectors. System costs will be minimized by extending the capabilities of existing commercial products.

COMMERCIAL APPLICATIONS:

The proposed system can be further developed to provide real time, feedback control of particle size, speed and distribution in thermal spray application systems. The proposed camera technology also lends itself to high speed imaging pyrometry for temperature studies of fast phenomena. Other applications include combustion and fuel injection studies, ink jet spray analysis, wind tunnel studies for aerodynamics and studies for a number of other spray related phenomena.

FY1999 Phase 1 Award Winner

TOPIC: 8.12 Intelligent and Distributed CAD

SUBTOPIC: 8.12.3T/CC Green Engineering Concepts for Next Generation Vehicles

TITLE: Green Engineering Concepts

NIST OU: 820

FIRM: Thar Designs, Inc.

730 William Pitt Way

Pittsburgh, PA 15238

PRINCIPAL INVESTIGATOR: Lalit Chordia

412-826-3939

AWARD AMOUNT: $74,950

ABSTRACT:

Montreal Protocol requires that ozone-depleting gases such as clorofluorocarbons (CFC) should no longer be used soon. As an example, automobile air conditioning systems, with over 40-45 millions cars being fitted with air conditioners every year, represent a major source of refrigerant emissions to the environment. Replacing freon with carbon dioxide would be the ideal situation as was done in the early part of this century. This problem represents a unique opportunity to design and develop a new compressor based on Green Engineering. Green Engineering is the encapsulated applied research and design of systems that can impact the ecology at a significant level.

Designers have to utilize a vast array of design tools in order to develop a given product. The design team involved in Green Technologies has in addition to the typical design process: layer's of scientific, regulatory, and ethical data to address. Green Technology Designers need a Coupled Component Design System that has an accessible source of information related to their project, and the most current, authoritative, and extensible knowledge base with which to focus the design process. The design, and analysis tool set must be advanced and scaleable in order to disseminate and incorporate each component to its specification within the design. A collaborative exchange of information is extremely necessary for the design team to assure a timely development of design tools admission into the design repository.

COMMERCIAL APPLICATIONS:

With over 40-45 million air conditioned cars being made each year, even a small market share will make a significant dent in the emissions to the environment. The long-term market potential for compressors in the automotive industry is over $1.2 billion dollars annually, and this is expected to grow as the demand for cars fitted with air conditioners grows every year. This product is especially attractive in the developed countries due to environmental considerations and in third world countries due to the high cost of HCFC's. Once this process is proved for this application, it can be extended to other applications.

FY1999 Phase 1 Award Winner

TOPIC: 8.13 Infrastructure for Distributed Electronic Commerce

SUBTOPIC: 8.13.5T Natural Language Interface to 3-D Character Animations

TITLE: Conversational 3-D Character On-Line Agents

NIST OU: 890

FIRM: Seamless Solutions, Inc.

3504 Lake Lynda Drive, Suite 390

Orlando, FL 32817

PRINCIPAL INVESTIGATOR: Edward Sims

407-737-7309

AWARD AMOUNT: $74,707

ABSTRACT:

This SBIR Phase 1 project will demonstrate the feasibility of real-time, natural language interaction with an Internet-based 3D Virtual Human Agent that can demonstrate the features, operation, maintenance, and assembly of new products. This project will be: (1) developed to operate on low-cost PC hardware; (2) demonstrated in a standard Internet browser environment, using VRML 97; (3) fully consistent with the standards being developed by the Humanoid Animation (H-ANIM) working group of the VRML consortium; and (4) coordinated with the initiatives being undertaken by the Natural Language Processing Animation (NLP-ANIM) and other working groups dedicated to developing related standards. In Phase 1, we will design and integrate a Test Bed that leverages existing hardware and software, and will perform trade studies on the proposed architecture, using a simple operator or maintenance task. We will also demonstrate the ability to compose new, more complex character interactions from basic library animations. In Phase 2, we will use the research results and Test Bed from Phase 1 to develop a fully operational prototype of a Natural Language Processing/Virtual Human (NLP/VH) agent that (1) demonstrates the features, operation, maintenance, and assembly of a product; and (2) learns new tasks by composing them from a library of basic animations.

COMMERCIAL APPLICATIONS:

A Conversational 3D Character On-line Agent, that demonstrates products and tasks in response to natural language commands, can enable new modes of communicating product information over the Internet. By providing a faculty to learn new, composite actions, the VH Agent will be adaptable to new tasks and situations. When linked with on-line learning, distributed manufacturing, e-commerce, and entertainment software, the same NLP/VH Agent can provide an immediacy and flexibility of interaction not available with "point and click" or joystick type controls.

FY1999 Phase 1 Award Winner

TOPIC: 8.13 Infrastructure for Distributed Electronic Commerce

SUBTOPIC: 8.13.10T Displays for Learning Technologies and Information Dissemination

TITLE: Evaluation and Integration of a Novel Volumetric 3D Display Technology

NIST OU: 890

FIRM: Genex Technologies, Inc.

10605 Concord Street, Suite 500

Kensington, MD 20895

PRINCIPAL INVESTIGATOR: Jason Geng

301-962-6565

AWARD AMOUNT: $75,000

ABSTRACT:

Genex Technologies, Inc. (GTI) has recently made a breakthrough in high-resolution volumetric three-dimensional (3D) display technology by offering volumetric 3D display capability of over 8,000,000 voxels. Capitalizing upon our success, and facing new challenges brought by this innovation, we propose herein a Phase 1 SBIR program to: (1) perform a thorough evaluation of this novel volumetric 3D display technique in the context of human-display interface standards; and (2) develop a prototype volumetric 3D display device that integrates the powerful volumetric 3D capability with image storage and interactive user interface functions to enhance knowledge acquisition, comprehension, and management.

COMMERCIAL APPLICATIONS:

The commercial market for true 3D display systems is sizable (the market for compatible 2D display was about $22 billion/year in 1995 and is continuously growing) and applications are enormous, including both military (e.g., air traffic control, pilot training, battle management, submarine navigation, telemedicine, etc.) and commercial (e.g., 3D TV, virtual reality, computer aided design, visualization of multidimensional data, medical imaging, surgery assistance, education, scientific computing, video games, stadium displays, etc.). The 3D display system will provide a new level of realism and literally add a new dimension to the dynamic interaction between human, display, and computers.

FY1999 Phase 1 Award Winner

TOPIC: 8.13 Infrastructure for Distributed Electronic Commerce

SUBTOPIC: 8.13.11T Security Requirements Analysis, Methods and Tools

TITLE: Security Requirements Analysis, Methods and Tools

NIST OU: 890

FIRM: VDG, Inc.

6009 Brookside Drive

Chevy Chase, MD 20815

PRINCIPAL INVESTIGATOR: Serban Gavrila

301-975-4343

AWARD AMOUNT: $74,972

ABSTRACT:

The research proposed herein is intended to solve two problems, namely (1) to define a method for the analysis of protection profiles (e.g., those of the Common Criteria for IT Security, FIPS 140 series) for distributed systems, networks, and their subsystems in a precise and systematic manner; and (2) to provide a set of automated tools to support profile development and analysis. Precise analysis methods and tools for profile requirements and components have not been available because a formal basis for classifying and analyzing the dependencies among these requirements and components does not exist to date. Furthermore, a systematic way of composing security components into a profile in a manner that enables the demonstration of their effectiveness in countering a specific set of threats is also lacking. While useful in practice, extant profile development tools are in effect simple aids for the display, manipulation, storage, and formatting of textual requirements. These tools do not satisfy our profile development, analysis and effectiveness goals. The overall objective of this project is to develop a precise method and a set of tools for the analysis and synthesis of protection profiles, and for the specification of security targets based on a wide variety of security-requirement sets of different sizes and complexity.

COMMERCIAL APPLICATIONS:

The profile development and analysis method and tools, when fully implemented, will provide a significant measure of confidence in consistency, completeness, and effectiveness of protection profiles and security targets. We envision that the method and tools would be used for the development and analysis of new protection profiles by both private industry, government, and commercial security certification services both in the U.S. and internationally, for both the Common Criteria and other, more specialized, security standards, e.g., cryptographic frameworks.

FY1999 Phase 1 Award Winner

TOPIC: 8.15 Measurement & Standards for Composite Materials

SUBTOPIC: 8.15.1T Methods & Tools to Support Composite Materials for Civil Infrastructure

TITLE: Low Cost Renewable Resin for Pultruded Products

NIST OU: 470

FIRM: Composite Products, Inc.

9417 South Broadway, Suite 110

St. Louis, MO 63125

PRINCIPAL INVESTIGATOR: John Unser

314-638-6525

AWARD AMOUNT: $74,977

ABSTRACT:

One of the fastest growing industries is the civil infrastructure. Composites usage represent only a small percentage of the civil infrastructure market. In 1997, composite material shipments to this market were 700 million pounds. In just September of 1998, steel shipments in this market were 2.4 billion pounds. One of the main reasons for the small penetration of composites into this market is that they are too expensive. Two of the major cost drivers for composites are labor and raw materials. Labor costs can be reduced significantly through the use of pultrusion, which is a continuous low cost fabrication method for composites. However, there has not been much focus on the development of low cost, high performance raw materials for use on composites. The use of renewable raw materials such as Epoxidized Soybean Oil in resin formulations offer low cost ($.50 per pound) raw materials. Another problem with composites is that they are not ductile, therefore they fail catastrophically. Epoxidized Soybean Oil in resin formulations offer damage tolerance, ductility, and flexibility. Composite Products Inc. (CPI) and the University of Missouri - Rolla have teamed to propose to develop a new resin system for pultrusion base on this renewable raw material source. Preliminary work indicates that a pultrudable resin system can be made that is more ductile without much loss in strength.

COMMERCIAL APPLICATIONS:

The potential uses of pultruded composite products that are strong, damage tolerant, and flexible are numerous. CPI envisions implementation in applications where catastrophic failure could be life threatening such as hand railings in industrial sites, safety rails for off shore platforms, deck railing systems for boats, and road barriers. CPI is currently building several all composite bridges in Missouri. CPI will focus on the development of road barriers, which is a natural extension of the bridge effort.

FY1999 Phase 1 Award Winner

TOPIC: 8.15 Measurement & Standards for Composite Materials

SUBTOPIC: 8.15.2T Flow Detection Method for FRP Composites Used to Repair Concrete and Masonry

TITLE: NDE of FRP Repairs for Concrete and Masonry

NIST OU: 860

FIRM: Texas Research Institute Austin, Inc.

9063 Bee Caves Road

Austin, TX 78733-6201

PRINCIPAL INVESTIGATOR: George Matzkanin

512-263-2101

AWARD AMOUNT: $74,997

ABSTRACT:

Adhesively bonding fiber reinforced polymer (FRP) materials to concrete and masonry structural components has emerged as a valuable way to repair America's aging infrastructure. Widespread use of this technology is hampered, however, by the current inability to qualify such repair.

Texas Research Institute Austin, Inc. (TRI/Austin) will determine the capabilities and limitations of various NDE methods for detecting defects in FRP bonded repairs of concrete infrastructure. TRI/Austin operates the Nondestructive Testing Information Analysis Center (NTIAC) for the U.S. Department of Defense. The in-house capabilities gained by running NTIAC make us uniquely qualified to achieve the proposed effort.

In Phase 1, TRI/Austin will perform a complete information collection and critical review to determine which NDE methods offer the most promise for detecting defects in FRP repairs. This review will recommend the four most promising NDE techniques, and vendors qualified to complete them. Samples containing artificially introduced defects, such as delaminations, debonds, voids, and resin rich areas will be sent to these four vendors for laboratory inspections. All data collected throughout the project will be analyzed and reported to NIST.

Phase 2 work will include field development of the most promising technique(s), as well as developing inspection procedures and calibrations standards.

COMMERCIAL APPLICATIONS:

Composite materials are becoming more and more common. They are being used in such applications as aeronautics, automobiles, and boats. The technology used in this project will be able to evaluate such items as composite masts and fiberglass panels.

FY1999 Phase 1 Award Winner

TOPIC: 8.17 Microelectronics Manufacturing Infrastructure

SUBTOPIC: 8.17.1T Scanning Microwave Microscope for 2-D and 3-D Dopant Profiling of Semiconductors

TITLE: Nanometer-Scale Semiconductor Analysis with Tunable Microwave Microscopy and Spectroscopy

NIST OU: 810

FIRM: Atolytics, Inc.

545 Orlando Avenue

State College, PA 16803-3479

PRINCIPAL INVESTIGATOR: Gregory McCarty

814-863-8220

AWARD AMOUNT: $75,000

ABSTRACT:

We propose to develop tunable microwave frequency scanning tunneling microscopy and spectroscopy for 2-D and 3-D dopant profiling of semiconductors. For Phase 1, we will use existing state-of-the-art instrumentation at Penn State. We will have access to a wide range of semiconductor samples which will undergo complementary analyses using the current standard technologies. We will be partnering with a leading analytical services company for this purpose. Our tunable microwave frequency scanning tunneling microscopes are extremely versatile in terms of measuring linear and nonlinear, scalar and vector, and transmitted and reflected signals over a wide range of biases and frequencies (0-20 GHz). In Phase 1, we will measure tunneling impedance as a function of frequency and bias. We will determine which measurements are information-rich in terms of dopant profiling. In subsequent work, we will make these measurements quantitative. Through partnerships, we have ready access to samples, markets, and future technologies as they are being developed.

COMMERCIAL APPLICATIONS:

Nanometer-scale analyses for the electronics, communications, and biotechnology industries. The commercial applications of this work will be developed simultaneously through ongoing partnerships.

FY1999 Phase 1 Award Winner

TOPIC: 8.17 Microelectronics Manufacturing Infrastructure

SUBTOPIC: 8.17.5T Advanced Chemical Modeling and Simulation Tools for Semiconductor Processing

TITLE: Advanced Chemical Modeling and Simulation Tools

NIST OU: 830

FIRM: Reaction Design

11436 Sorrento Valley Road

San Diego, CA 92121

PRINCIPAL INVESTIGATOR: Erik Egan

619-550-1920

AWARD AMOUNT: $74,391

ABSTRACT:

Chemistry is at the heart of most semiconductor and materials manufacturing processes. Models that describe the interaction between chemistry and transport in reactors are a core technology for improving production efficiency, quality control and operating costs. A key input to these models is a reaction mechanism and associated chemical data. Today, synthesis of these mechanisms is a difficult, time-consuming task and there are few support tools. This proposal presents a plan for development of a prototype environment that incorporates: chemical databases, uncertainty analyses, chemically reacting flow simulation, visualization and data analysis. The goal is to develop a commercially viable system that will reduce the time needed to generate chemical mechanisms and analyze the results of reacting flow simulations. Five tasks are proposed: (1) review methods for generating mechanisms; (2) design a software architecture and database management system for storing chemical species, their chemical properties, reaction steps, mechanisms, uncertainties and documentation; (3) implement a prototype system (based on the NIST CKmech code) that simplifies access to the information base; (4) integrating into CHEMKIN reaction modeling environment algorithms for sensitivity and uncertainty analysis; and (5) define a post-processing analysis system.

COMMERCIAL APPLICATIONS:

One of the largest challenges in the semiconductor industry today is the move to larger wafers and smaller features while also introducing new material systems. Chipmakers will reduce resulting process development costs by using simulation tools from this research to gain more information with fewer experimental wafers, while freeing production capacity for processing saleable material. They will also speed process optimization by replacing time consuming experiments with faster simulations to reach high-yielding processes quickly, shortening time-to-market. Their equipment and chemicals suppliers will likewise use the software for faster, cheaper reactor and chemical systems development to accelerate overall technology evolution. The entire industry will apply the product to understand how to improve efficiency and reduce emissions of harmful waste chemicals. Such uses readily extend to combustion and chemical processing industries.

FY1999 Phase 1 Award Winner

TOPIC: 8.17 Microelectronics Manufacturing Infrastructure

SUBTOPIC: 8.17.7T High Temperature Thin Film Insulation

TITLE: Novel High Temperature Insulators for Thin Film Thermocouples

NIST OU: 830

FIRM: ATMI, Inc.

7 Commerce Drive

Danbury, CT 06810

PRINCIPAL INVESTIGATOR: Frank DiMeo, Jr.

203-794-1100

AWARD AMOUNT: $75,000

ABSTRACT:

Thin film thermocouple technology for real-time, high-temperature (1000C), distributed thermometry spans a wide range of commercial application areas, including semiconductor manufacturing and combustion engine feedback. At present, a lack of suitable high-temperature thin film insulators, required to provide an adhesive interface we well as an electrical and chemical barrier between the substrate and the thermo-elements, severely hinders widespread implementation of this technology. Compounds from the MgO-SiO2-Al203 ternary system offer the opportunity to overcome the limitations of conventional insulators. These compounds are chemically compatible with silicon, have high resistivity at elevated temperatures, and offer a range of coefficients of thermal expansion. Metal organic chemical vapor deposition (MOCVD) of complex oxides is an attractive fabrication method because of its ability to cover large areas with high quality films and, coupled with the ability to coat complex shapes, can conformally encapsulate thin film thermocouples for improved robustness. In Phase 1, MgO and MgAl204 films will be deposited by MOCVD on silicon substrates and fully characterized, including electrical behavior at elevated temperatures. In Phase 2, film performance will be optimized, full encapsulation of thin film thermocouples will be examined, and the deposition process will be extended to insulator films such as Mg2Al3(AISi)5018.

COMMERCIAL APPLICATIONS:

The potential commercial applications of thin film insulator compounds from the MgO-Si02-Al203 ternary system include high temperature insulators for silicon wafer based thermometry using thin film thermocouples, gas turbine engine thermometry, and barriers/buffer layers for advanced semiconductor devices.

FY1999 Phase 1 Award Winner

TOPIC: 8.17 Microelectronics Manufacturing Infrastructure

SUBTOPIC: 8.17.8T Measurement of Trace Alpha Radiation in Polymeric Microchip Material

TITLE: Measurement of Trace Alpha Radiation In Polymeric Microchip Material

NIST OU: 840

FIRM: Fayette Environmental Services, Inc.

120 E. Davis Street, P.O. Box 21

Fayette, MO 65248-0021

PRINCIPAL INVESTIGATOR: Rhys N. Thomas

660-248-1911

AWARD AMOUNT: $75,000

ABSTRACT:

The reduction of alpha particle emission induced soft error upset has been identified in the industry association's National Technology Roadmap for Semiconductors as a major concern. However, the measurement of ultratrace alpha radiation levels is difficult, and has become a source of conflict between materials suppliers and microchip manufacturers. Development of an inexpensive standardized test method has been solicited to allow for accurate analysis to a detection limit far below the current low-alpha standards. Not only will this alleviate the misunderstandings between suppliers and users, but also will permit further research into the source and removal of the ultratrace contamination.

The process to be developed under this proposal utilizes three unique principles in order to provide an improvement in detection limit of more than a factor of 50 over the best available technology. First, this process evaluates volumetric content of alpha activity rather than surface content, greatly increasing the effective size of the sample. Second, it requires no chemical separations or processes to isolate trace alpha emitters from the encapsulant material. Third, it utilizes a unique, digital counting system that provides precise selectivity for alpha decay events, thus eliminating background radiation and improving alpha detection sensitivity.

COMMERCIAL APPLICATIONS:

The method for ultratrace detection of alpha emissions developed under this proposal will be of value not only to the semiconductor industry but also for environmental monitoring at various governmental sites formerly used for nuclear weapons research or uranium production. The proposed device will be economical enough to allow surveying of contamination fields to map plume development.

FY1999 Phase 1 Award Winner

TOPIC: 8.17 Microelectronics Manufacturing Infrastructure

SUBTOPIC: 8.17.9T Advanced Ion Beam Methods for Nanotechnology

TITLE: Highly Charged Ions - A New Tool for Nanotechnology

NIST OU: 840

FIRM: Charles Evans & Associates

301 Chesapeake Drive

Redwood City, CA 94063

PRINCIPAL INVESTIGATOR: Kuang Jen Wu

650-369-4567

AWARD AMOUNT: $74,974

ABSTRACT:

The goal of this proposal is to develop advanced mass spectrometry instrumentation based on the use of slow, highly charged ion (HCI) such as Xe44+ or Au69+. The competitive characteristics of this excitation source for secondary ion mass spectrometry (SIMS) arises from the unique power density of ~1E14 W/cm2 that can be delivered into a nanometer-scale surface area. Secondary ion yields in highly charged ion SIMS are increased by a factor of

100 - 1000 as compared to conventional SIMS. This improvement enables chemical structure analysis on a 10 nm length scale through integration of coincidence counting. The proposed research will determine the feasibility of Highly Charged Ion SIMS for industrial applications in the semiconductor and biotech industries. We propose to target (1) advanced metallization: sub-micron copper lines on silicon; and (2) biomolecular assemblies: interface bonding properties as examples where available techniques have been insufficient in addressing critical industry needs. Phase 1 research will be performed at Lawrence Livermore National Laboratory where highly charged ion technology has been developed for about a decade.

COMMERCIAL APPLICATIONS:

Analytical instrumentation for chemical analysis of nanometer scale surface features.

FY1999 Phase 1 Award Winner

TOPIC: 8.17 Microelectronics Manufacturing Infrastructure

SUBTOPIC: 8.17.10T High Precision Manufacturing of Rockwell Diamond Indenters

NIST OU: 820

TITLE: Innovative Manufacturing Methods for Diamond Indenters

FIRM: Gilmore Diamond Tools, Inc.

43 Roger Williams Avenue

East Providence, RI 02916

PRINCIPAL INVESTIGATOR: Michael Mihalec

401-438-0717

AWARD AMOUNT: $75,000

ABSTRACT:

Due to the inherent properties of Natural Diamond, indenters produced by traditional manufacturing methods yield unacceptable variations in their geometric profiles. It will become our objective to repeatedly reproduce Rockwell indenters with tighter geometric tolerances than those currently available for standardization and traceability. Our primary focus will be the implementation of advanced grinding systems, coupled with experimental techniques and variations in grinding wheel specifications. The variables will translate directly into documented test results directed towards minimal variations in cone angle and radius measurements. Additional areas of evaluation will monitor surface finish, and interpret measurement results gathered both on site and though working relationships with Government Facilities and Universities.

COMMERCIAL APPLICATIONS:

Diamond indenters produced utilizing advancements in manufacturing technologies would represent an available source of calibration grade indenters with direct traceability to NIST and ISO standards. These indenters would be available to testing laboratories, Test Block manufacturers, Hardness Testing Machine manufacturers, and facilities dependent upon accurate and repeatable hardness testing results, with direct traceability to National Standards.

FY1999 Phase 1 Award Winner

TOPIC: 8.18 Microfabrication and Micromachining

SUBTOPIC: 8.18.1T Ultra-Sensitive Atomic Force Microscope Cantilevers

TITLE: Ultra-Sensitive Torsional Oscillators for Scanning Probe Microscopes

NIST OU: 810

FIRM: Xidex Corporation

8906 Wall Street, Suite 105

Austin, TX 78754

PRINCIPAL INVESTIGATOR: Validmir Mancevski

512-339-0608

AWARD AMOUNT: $75,000

ABSTRACT:

Xidex proposes to team with UT Austin to develop a new type of ultra sensitive force sensor suitable for use with scanning probe microscopes. Ultra sensitive force detection will be enabled by using high-Q silicon multiple torsinal oscillators. Our strategy to attain and surpass a force sensitivity of 1016N/Hz1/2, which is required to measure extremely small electro-dynamic forces, involves two main thrusts: (1) utilizing double- and multiple-torsional oscillator modes, which can enhance oscillator quality factor Q by a factor of 100 or more; and (2) replacing ultrathin silicon-nitride (amorphous) cantilevers with single-crystal silicon structures, which can further enhance the Q by a similar or greater factor. Phase 2 will focus on improving the repeatability and scalability of the batch fabrication process, thus enabling incorporation of ultra-sensitive cantilevers into planed OEM modules and sale of cantilevers themselves to end users of scanned probe microscopy tools and instruments.

COMMERCIAL APPLICATIONS:

Targeted commercial applications include magnetic force microscopy (MFM), magnetic force resonance microscopy (MFRM), lateral force microscopy (LFM), and scanning potentiometry. Two commercial embodiments of the technology will be evaluated: (1) sensing components, bundled with appropriate software, for sale to OEMs of laboratory instrumentation; and (2) integration of the technology into our own stand-alone tools for sale directly to end users. The channel we pick will depend on the application or applications that have the greatest commercial potential.

FY1999 Phase 1 Award Winner

TOPIC: 8.18 Microfabrication and Micromachining

SUBTOPIC: 8.18.5T Three-Dimensional Imaging System for Low Activity Brachytherapy Sources

TITLE: High Resolution, 3-D, Digital Image Calibration System for Brachytherapy Sources

NIST OU: 840

FIRM: Industrial Quality Inc.

640 E. Diamond Avenue, Suite C

Gaithersburg, MD 20877-5323

PRINCIPAL INVESTIGATOR: Harold Berger

301-948-2460

AWARD AMOUNT: $75,000

ABSTRACT:

Improved methods are needed to calibrate the radiation emission uniformity of small radioactive sources used for radiation therapy. Improvements are needed in terms of spatial resolution and ease of use. A novel radiation imaging instrument is proposed to be developed for use in mapping the three-dimensional radiation levels emitted from relatively low activity brachytherapy sources. A scintillating glass-CCD camera system offers the potential for sensitive, high resolution imaging in a geometry what will provide a full three-dimensional map of the emitted radiation, in a measurement time estimated in minutes. The developed instrument will permit measurements to be made in an efficient manner, in an operational mode much simpler to use as compared to the cumbersome methods currently in use. The Phase 1 project is planned to demonstrate the feasibility of the imaging system and geometry and help determine if additional scintillators will be needed for the prototype instrument. The proposed radiation camera system clearly has the sensitivity needed for measurements/calibration of low activity sources. A major advantage of the proposed scintillator-camera system is the prospect for rapid, easy-to-use measurements that can be related to dose.

COMMERCIAL APPLICATIONS:

Multiple markets are foreseen for this efficient, radiation mapping scintillator-camera instrument. Instrument needs exist with manufacturers of small radioactive sources, with organizations that offer radiation calibration services and, particularly with the many radiation oncology centers that are the primary uses of brachytherapy sources. There are more than 1,500 radiation oncology facilities in the U.S. alone, representing a potential market of $75 million.

FY1999 Phase 1 Award Winner

TOPIC: 8.20 Photonics Manufacturing

SUBTOPIC: 8.20.1T Photonic Components/Systems Manufacturing Cost Reduction

TITLE: Materials Processing for Mass-Producible Distributed Photonic Amplifiers

NIST OU: 890

FIRM: Intelligent Fiber Optics Systems (IFOS)

1778 Fordham Way

Mountain View, CA 94040

PRINCIPAL INVESTIGATOR: Richard Black

650-967-4107

AWARD AMOUNT: $75,000

ABSTRACT:

Photonic systems offer enormous potential because of the extraordinary large bandwidth that they deliver. However, component cost dominated by optical amplifiers constrains their proliferation. Furthermore, a common problem is component loss including splitting-loss whereby signal strength per channel is reduced whenever a signal is split. For an economic and compact solution to this problem, there is the need for integrated-optic devices that combine splitting and amplification of light. Erbium-doped amplifiers have become well established in fiber form. However, their manufacture is today complex and costly. IFOS proposes to combine integrated-optic splitter fabrication with a new approach for manufacture of integrated-optic amplifiers. It will open up new application opportunities for amplifiers in subsystems intended for sensing, signal processing and communications. Our approach brings together processing technologies that are low-cost, low-temperature and lend themselves to high-volume production. In Phase 1, we will focus on materials processing and analyze, fabricate and characterize active-glass waveguide substrates for proof-of-concept demonstration of high gain-per-unit-length. In Phase 2, we will demonstrate active-ridge-waveguides and fabricate an optimized 1x2 lossless splitter and begin commercialization activities. IFOS has demonstrated its expertise in photonics including amplifiers and couplers/splitters, materials processing, business and marketing.

COMMERCIAL APPLICATIONS:

The IFOS low-cost, highly manufacturable, distributed photonic amplifier technology will significantly enhance performance of photonic systems in telecommunications, cable TV, Internet access and optical signal processing systems. A multiplicity of distributed, low-cost, low-gain amplifiers and splitters can be integrated on the same chip to perform cost-effective all-optical signal processing with improved signal-to-noise ratios. The fiber amplifier market is now over $500 million and is doubling every four years.

FY1999 Phase 1 Award Winner

TOPIC: 8.20 Photonics Manufacturing

SUBTOPIC: 8.20.4T In Situ, Noncontact Temperature Measurements of Semiconductors

TITLE: Noncontact Measurement of MBE Substrate Temperature

NIST OU: 810

FIRM: ARACOR

425 Lakeside Drive

Sunnyvale, CA 94086

PRINCIPAL INVESTIGATOR: Jonathan Kerner

408-733-7780

AWARD AMOUNT: $75,000

ABSTRACT:

There is a need to improve the reliability of semiconductor photonic devices, such as lasers, LEDs, photodetectors and modulators which are critical to the high-growth industries concerned with wireless and optical telecommunications, high speed networks, and imaging. The lack of accurate, in situ process control monitors during device fabrication can lead to defect generation and poor reproducibility of component parameters, such as film thickness and composition, which strongly impact device lifetime and performance.

To improve reliability, new deposition processes are being developed at low temperatures (150 to 450C) using molecular beam epitaxy (MBE). This Phase 1 project is designed to demonstrate the feasibility of using x-ray diffraction for the in situ, not-contact measurement of substrate temperature, a critical MBE processing parameter. The objectives will be to show that the x-ray measurement can yield a temperature accuracy of ±1C in the presence of substrate rotation, and to evaluate the effect of epitaxial films on the measurement. A breadboard instrument will be built to test the concept with GaAs substrates, and a collaboration with NIST to examine relevant samples and interfacing issues will insure a Phase 2 prototype which is compatible with the MBE processing chambers.

COMMERCIAL APPLICATIONS:

The main commercial applications are associated with epitaxial and thin film growth equipment processes including molecular beam epitaxy (MBE), rapid thermal processing (RTP) and chemical vapor deposition (CVD).

FY1999 Phase 1 Award Winner

TOPIC: 8.20 Photonics Manufacturing

SUBTOPIC: 8.20.6T Ultra-Hard/Sapphire Tools for Precision Machining

TITLE: Ultra-Hard Nanoceramic Tools for Precision Machining

NIST OU: 820

FIRM: Nanopac Technologies, Inc.

35 Hutchinson Road

Allentown, NJ 08501

PRINCIPAL INVESTIGATOR: Dr. Shih Chieh Liao

732-445-5627

AWARD AMOUNT: $70,000

ABSTRACT:

This Phase 1 project will result in wear-resistant nanoceramic cutting tools for use in ultraprecision machining operations. In previous research, we have discovered a method for producing fully dense, bulk ceramic materials which retain their nanoscale grain size. Characterization of these materials has demonstrated that the nanoceramics have exceptional wear resistance with an extremely fine surface finish. As an example, we have been able to produce nanograined ceramics with wear resistance that is 4x better than their micrograined counterpart. In this effort, we will apply our processing technique to produce bulk ceramic materials with grain sizes <100nm, densities >99%, and surfaces finishes below 50nm. We will then characterize these materials for their usefulness as ceramic cutting tools. We anticipate that the combination of ultrafine grain size and nearly full density will impart the required properties to this new generation of materials. In the Phase 2 effort, we will work with our partner, Tempo Technology Corp., to optimize the scale-up to produce large bulk samples and then to optimize the properties of the cutting tools for the best combination of wear resistance and toughness. The Phase 3 effort will address the manufacture and commercialization of specific nanoceramic cutting tools.

COMMERCIAL APPLICATIONS:

The nanoceramic cutting tools developed in this project are expected to replace diamonds in a variety of applications. In those cases where diamond interacts with the workpiece, we expect that the ceramic materials will exhibit better stability and lower reactivity. In addition, the nanoceramics are expected to exhibit many properties similar to diamond, such as cutting tool sharpness and wear resistance. Until now, there has been no suitable alternative to diamond for ultraprecision cutting operations. However, we expect that the nanoceramics will match many properties of diamond, and may actually exceed it in terms of toughness due to the retained nanograin size.

FY1999 Phase 1 Award Winner

TOPIC: 8.22 Integration of Manufacturing Applications

SUBTOPIC: 8.22.1T Next Generation Process Exchange Tools and Applications

TITLE: Integration of Manufacturing Applications Through Next Generation Process Exchange Technology

NIST OU: 820

FIRM: Intelligent Systems Technology, Inc.

2800 28th Street, Suite 306

Santa Monica, CA 90405

PRINCIPAL INVESTIGATOR: Azad Madni

310-581-5440

AWARD AMOUNT: $74,955

ABSTRACT:

The overall objective of this SBIR effort is to provide an easy-to-use generic PSL representation viewer and editor and a PSL Translator toolkit to facilitate development of translators. In addition, this project will also evaluate the adequacy of the organizational aspect of the current PSL ontology. A robust and complete common process representation is essential for application integration in a manufacturing environment. The PSL is positioned to fulfill that requirement. PSL is not used in any commercial product because of lack of good generic PSL tools. To this end, the proposed effort is directed to create a generic PSL representation viewer and editor for the users to review and modify process models stored in PSL format. The proposed effort will also create a PSL Translator architecture and toolkit that will speed up the development of translators for integrating various applications using PSL as the common language. The proposed scalable, web-based PSL Viewer and Editor architecture and the proposed symmetric modular design for the PSL Translator will make PSL easier to use and greatly reduce the effort in manufacturing application integration.

COMMERCIAL APPLICATIONS:

Commercial applications of this research include: (a) process exchange between different applications such as process design, workflow managers, project management tools, schedulers and process simulations; (b) supply chain integration and management; (c) enterprise resource planning; and (d) enterprise application integration.

FY1999 Phase 2 Award Winner

TOPIC: 8.7 Advanced Technology Program

SUBTOPIC: 8.7.1T Technologies for Large Area Electronic Materials and Devices

TITLE: 3-D Printing of Opto-Electronic Components on Flexible Substrates

NIST OU: 890

FIRM: Gemfire Corporation

2471 East Bayshore Road Suite 600

Palo Alto, CA 94303

PRINCIPAL INVESTIGATOR: Nigel Cockroft

650-849-6800

AWARD AMOUNT: $300,000

ABSTRACT:

The technique of screen printing has been demonstrated to be of practical benefit in numerous engineering applications. Over the past two decades, these benefits have been widely recognized by the electronics industry, as evidenced by the flourishing fields of screen-printed thick-film electronics. Multilayer circuits are now manufactured by the sequential deposition of conductive and resistive paste patterns and the deposition of solder bumps and epoxies to secure precisely mounted components. We propose to apply these advanced screen printing methods to large-area opto-electronic applications. In Phase 1, we demonstrated the feasibility of screen printing three-dimensional optical components on a flexible substrate using electroformed stencils, where feasibility was defined as being able to print fine-pitch 3-D optical features of precise dimension, and being able to print a second set of features over the first without damaging either. In Phase 2, we will develop several precision printing techniques required to demonstrate a multilayer device on a flexible polymer substrate for consumer-electronics display applications.

COMMERCIAL APPLICATIONS:

The ability to screen printing 3-D opto-electronic components on thin, flexible substrates will provide a powerful new way of manufacturing low-cost, large-area integrated optics. Used in conjunction with existing electronic printing capabilities, the proposed method will greatly accelerate the emergence of large-area opto-electronic devices. The technology is anticipated to enable numerous unexpected applications in thin-film electronics.

FY1999 Phase 2 Award Winner

TOPIC: 8.9 Manufacturing Engineering

SUBTOPIC: 8.9.7T Next Generation Process Exchange Tools and Applications

TITLE: A Framework for Building Information Translators

NIST OU: 820

FIRM: Knowledge Based Systems, Inc.

1408 University Drive East

College Station, TX 77840

PRINCIPAL INVESTIGATOR: Florence Tissot

409-260-5274

AWARD AMOUNT: $299,760

ABSTRACT:

Today's manufacturing companies are concentrating their energy towards breaking the barriers between firms all along the supply chain to create a virtual enterprise whose goal is to operate as if the chain was a single entity. Breaking these barriers involves facilitating collaboration and communication at all levels of the enterprise. A key roadblock to this sort of facilitation is the need for a computer system interoperability that enables manufacturers and product suppliers to move and share information up and down the supply chain.

In this project, we propose to implement a framework for developing and maintaining an information translator for the entire supply chain. The translators generated by the framework will not only enable the exchange of properly formatted data, but will take into account the meaning of data during the translation. The key innovations of this project are: (1) the use of ontologies to enable information translation, (2) foundations for ontology harmonization, (3) semantic translation through inferences, and (4) automated generation and management of translators. The technology developed in this project will enable companies to cost- and time-effectively integrate their ERP and ERM systems with their suppliers' stand-alone software applications.

COMMERCIAL APPLICATIONS:

There is strong evidence for commercial application potential for the proposed technology in several different areas. The most promising area is the ERP application area that is lacking tools that facilitate rapid integration of ERP systems with other stand-alone software tools. The explosive growth in ERP systems is expected to continue for the next few years with a continued technology void for integration tools. The second and broader market segment is to facilitate the development of general purpose integration mechanisms through the use of ontology-driven translators.

FY1999 Phase 2 Award Winner

TOPIC: 8.10 Chemical Science and Technology

SUBTOPIC: 8.10.2T Strongly Coupled CFD Code for Modeling of Spray Combustion Systems

TITLE: Next Generation CFD Code for Spray Combustion Simulations

NIST OU: 830

FIRM: CFD Research Corporation

215 Synn Drive

Huntsville, Al 35805

PRINCIPAL INVESTIGATOR: M.G. Girdharan

205-726-4800

AWARD AMOUNT: $299,952

ABSTRACT:

Despite major advances in CFD technology over the past two decades, simulation of industrial spray combustion systems remains challenging due to difficulties in modeling various droplet physical phenomena and in dealing with the geometrical complexity. The proposed study will develop a 3-dimensional code incorporating advanced physical models for droplet transport/vaporization and spray combustion by using solution-adaptive unstructured meshes and efficient parallel algorithms.

The Phase 1 effort demonstrated proof-of-concept by developing a baseline spray dynamics module incorporating heat and mass transfer and coupling it with an existing unstructured reactive flow solver. Comparison of model predictions for non-evaporating and burning sprays with experimental data showed good agreement. In Phase 2, the code will be extended to include state-of-the art models for droplet physics, such as multi-component droplets; droplet-turbulence interactions; droplet deformation, breakup and collisions; soot and gaseous emissions; detailed chemical kinetics; and group combustion, and stochastic spray. Additionally, solution-adaptive meshing techniques and algorithm improvements will be incorporated into the code. As part of a verification study, the developed code will be subjected to a series of test cases for which analytical solutions are available. Comprehensive benchmark validation of the code will be performed against data being collected at the NIST Spray Combustion Facility. A variety of full-scale 3-D waste fuel furnace/incinerator simulations will be performed to demonstrate the capabilities of the code. Prof. Aswani Gupta of the University of Maryland and Prof. Clayton Crowe of Washington State University will be consultants during the Phase 2 project. Phase 3 commitments and endorsements have been obtained from Optomec, BMW--Rolls-Royce and Geo-Centers, Inc.

COMMERCIAL APPLICATIONS:

The computer code developed under this study will be a valuable design and analysis tool to maximize the operating efficiency of spray combustion systems and to reduce the formation and release of harmful emissions. This software will have applications in gas turbine and rocket engine combustors, furnaces, evaporative cooling systems, particle separation systems, fire protection systems, chemical/process industries, and particle/dust cleaning systems used in microelectronic applications.

FY1999 Phase 2 Award Winner

TOPIC: 8.10 Chemical Science and Technology

SUBTOPIC: 8.10.6T New Technology Detectors for Analytical X-ray Spectometry

TITLE: New Technology EDS Detectors for X-ray Microanalysis

NIST OU: 830

FIRM: Photon Imaging, Inc.

19355 Business Center Dr. Suite 8

Northridge, CA 91324

PRINCIPAL INVESTIGATOR: Jan Iwanczyk

818-709-2468

AWARD AMOUNT: $300,000

ABSTRACT:

The goal of the proposed work is to develop a novel detector for analytical spectrometry having large active area, high-energy resolution and capable of operating at high counting rates. The proposed detector will be specifically designed for x-ray microanalysis to provide orders of magnitude advancement in the performance over conventional energy dispersive systems. During the Phase 1 effort of this project, we successfully designed, fabricated, and demonstrated a ~2cm2 silicon drift detector (SDD) array. All of the goals of Phase 1 were met, and most were significantly exceeded. Accomplishments included development of a closely spaced array of four 0.5 cm2 SDD elements. Energy resolution of 143 eV FWHM at 5.9 keV was achieved on the best device. All four devices produced energy resolution below 200 eV FWHM. Importantly, these results were obtained at relatively short peaking times and additionally the detectors do not require cryogenic cooling to obtain this performance.

In Phase 2, we will develop a prototype x-ray spectrometer for insertion into an electron microscope. The prototype will include the finalized detector array of up to four elements based upon the Phase 1 study. Each element will be capable of attaining electronic noise of <10 e- rms at peaking times on the order of 100 ns, allowing throughput rates exceeding 106 cps each. These advances will have a remarkable impact on reducing the acquisition time for 2-dimensional compositional mapping. The prototype system will be deployed for evaluation at NIST in one of the scanning electron microscope instruments.

COMMERCIAL APPLICATIONS:

The proposed new detectors will lead to significant performance improvements and lower cost systems. Elimination of the liquid nitrogen, combined with the low cost of silicon planar processing, will allow construction of affordable, small mass, low power consumption x-ray analytical systems. These new devices will replace many existing detectors based on cryogenic Si(Li) and High Purity Germanium, used in many commercial (e.g., microanalysis, x-ray fluorescence, x-ray diffraction, medical imaging) and scientific (nuclear, high energy physics, synchrotron radiation experiments) applications. Other new applications are possible for use in hand-held, portable field instrumentation.

FY1999 Phase 2 Award Winner

TOPIC: 8.11 Physics

SUBTOPIC: 8.11.14T Liquid-Nitrogen-Cooled Electrical Substitution Radiometer

TITLE: Advanced Absolute Radiometers Using Superconducting Transition Thermometers

NIST OU: 840

FIRM: CRI, Inc.

80 Ashford Street

Boston, MA 02134

PRINCIPAL INVESTIGATOR: Peter Foukal

617-787-5700

AWARD AMOUNT: $299,964

ABSTRACT:

In our Phase 1 work we were able to replicate and build on recent results at NIST with superconducting transition (SCT) thermometers, which suggested that dramatic improvements may be achieved in detectivity and range of application, of cryogenic electrical substitution radiometers. Cryo-ESR's are widely used as the most accurate absolute standards of radiative flux and irradiance. In Phase 2, we will focus on the additional research required to demonstrate that the advantages of SCT thermometry can be translated into: (a) LN2-cooled ESR's of comparable accuracy, but easier accessibility, than conventional, LHe-cooled instruments; (b) LHe-cooled ESR's capable of improved detectivity for detector calibrations in the aerospace industry; and (c) more stable pyrheliometers operating at 90 K for space-borne monitoring of radiations in solar total and ultraviolet irradiance. This research will include development of high-Tcsuperconducting heater leads having low thermal conductance, of an SCT thermometer based on thin metal films with Tc between 2-4 K, and characterization of a prototype LN2-cooled ESR through intercomparison with LHe-cooled ESR's at CRI, and calibration at the NIST HACR facility. CRI is the world's leading manufacturer of cryo-ESR's, and identifies total domestic and foreign markets of $10-15 M for this important new technology if the Phase 2 objectives in accuracy and system detectivity can be met.

COMMERCIAL APPLICATIONS:

(1) LN2-cooled electrical substitution radiometers for absolute measurement of light flux and irradiance, of similar accuracy, but more widely accessible, and less expensive to operate, than conventional LHe-cooled electrical substitution radiometers.

(2) LHe-cooled electrical substitution radiometers capable of ten times higher detectivity than conventional cryo-ESR's, for more widely useful aerospace detector calibrations.

(3) More stable pyrheliometers for NOAA or NASA monitoring of total and UV solar irradiance from space, in global change studies.

FY1999 Phase 2 Award Winner

TOPIC: 8.12 Materials Science and Engineering

SUBTOPIC: 8.127T/CC Process Monitoring and Control of Composites Processing

TITLE: Optical Fiber Devices for Composite Process Monitoring

NIST OU: 850

FIRM: F&S, Inc.

P.O. Box 11704

Blacksburg, VA 24062-1704

PRINCIPAL INVESTIGATOR: Paige Furrow

540-953-4282

AWARD AMOUNT: $275,000

ABSTRACT:

The primary objective of the Phase 1 program was the development of optical fiber devices and cost-effective signal conditioning systems to produce commercially available composite process monitoring systems. The tasks successfully completed during the Phase 1 effort are as follows: (1) examined the performance requirements of the optical fiber devices and demodulation systems for FT-IR- and fluorescent-based process monitoring systems, (2) fabricated special high-index fiber to operate in the near infrared (NIR) that is compatible with standard fiber optical connection components, (3) designed high-index optical fiber compatible grating fabrication that maintains optical transmission quality in the desired wave-length ranges, (4) designed and fabricated a prototype optical launch system for use with FT-IR systems to monitor epoxy resin cure, (5) designed and fabricated a prototype grating-based optical fiber sensor to monitor resin flow during composite processing, (6) investigated sensor elements for fluorescent applications, (7) designed and constructed cost-effective signal conditioning systems, and (8) demonstrated prototypes at F&S and NIST. The objective of the proposed Phase 2 program is to build upon the success of the Phase 1 effort and produce commercially available cure monitoring instrumentation based on patented F&S technology.

COMMERCIAL APPLICATIONS:

The inherent advantages of on-line and development stage process monitoring made possible using fiber optic systems will enable significant market penetration in the composite industry where structural performance is of major importance. The optimization of curing processes will lead to greater cost-savings; this makes optical fiber instrumentation attractive to composite manufacturers. The multi-billion dollar composite markets include the (1) aerospace, (2) automotive, (3) sporting goods, (4) heavy industry, (5) infrastructure, (6) oil and gas, and (7) government and academic research laboratories. Based on the initial market and competition analysis performed during Phase 1, the F&S team is actively targeting select market opportunities with intent to provide cost-effective process monitoring sensors to composite manufacturers.

FY1999 Phase 2 Award Winner

TOPIC: 8.12 Materials Science and Technology

SUBTOPIC: 8.12.11T Device and Technique for Measurement of Thermal Conductivity of Ceramic Powders

TITLE: High-Temperature Thermal Conductivity Measurements of Ceramic Powders

NIST OU: 850

FIRM: METSYS

P.O. Box 254

Millwood, VA 22646

PRINCIPAL INVESTIGATOR: Daniel R. Flynn

540-837-2186

AWARD AMOUNT: $275,000

ABSTRACT:

It is proposed to develop an advanced field apparatus for measuring the thermal conductivity of ceramic powders over the range of temperatures from room temperature to 1500 to 2500 K, depending upon the particular material and its compatibility with other materials. The apparatus will have the capability to carry out fully automated thermal conductivity measurements, by transient or steady-state means, under controlled gaseous environments and will be equipped with associated software to compute the thermal conductivity of the ceramic particle material from the data taken on powders. The specific objectives of the Phase 2 effort are: finalize the design of the prototype field apparatus for determination of the thermal conductivity of ceramic powders of mixtures, including construction drawings and selection of all instrumentation; develop software for experimental control, data acquisition, and data analysis for the prototype field thermal conductivity apparatus; further review available correlations and models relating the thermal conductivity of powders and mixtures to the properties of their constituents, and write appropriate software for use with the prototype field thermal conductivity apparatus; and build and test the prototype field thermal conductivity apparatus.

COMMERCIAL APPLICATIONS:

The apparatus design that is being developed, along with the software that will be developed for use with the apparatus, will provide the thermal spray industry with a valuable tool that can be used to select feedstock, based upon its thermal conductivity and other properties, and to optimize the thermal spraying process. The apparatus will be sufficiently inexpensive, and easy to operate, that it can be used by suppliers of feedstock, companies that apply thermally sprayed coatings, and researchers. In addition, the apparatus will be very useful for determining the thermal conductivity of powders used for other purposes, such as thermal insulation or formation of ceramic parts by various manufacturing processes.

FY1999 Phase 2 Award Winner

TOPIC: 8.13 Building and Fire Research

SUBTOPIC: 8.13.4T Low-Cost, Smart Vibration Sensors

TITLE: Low-Cost, Smart Vibration Sensor Utilizing CIFMEMS Technology and Postmolded-Plastic (PMP) Packing

NIST OU: 860

FIRM: OPTICAL E.T.C., Inc.

3077-K Leeman Ferry Road

Huntsville, AL 35801

PRINCIPAL INVESTIGATOR: Jon Geist

301-774-7280

AWARD AMOUNT: $299,992

ABSTRACT:

The feasibility of a very lost cost approach to producing smart amplication-specific vibration sensors will be investigated. The approach consists of: (1) fabricating integrated circuit wafers containing vibration sensor precursors and signal processing electronics at a commercial Application-Specific Integrated-Circuit (ASIC) foundry service in a completely standard CMOS process; (2) processing the completed wafers to convert the sensor precursors into functional sensors on dies suitable for postmolded-plastic (PMP) packaging; and (3) packaging the dies at a commercial PMP packaging service. Sensor system protyping will be carried out with low-cost multi-project wafer runs and a full-wafer layout will be designed when prototyping is completed. Low-cost test wafers that simulate the sensor-wafer layout will be fabricated and run through steps 2 and 3 to verify that they are working properly. Then a small batch of full wafers will be run through steps 1, 2, and 3. The results will be somewhere between 10,000 and 40,000 single-chip demonstration vibration-sensor systems for testing by potential customers for custom systems.

COMMERCIAL APPLICATIONS:

There is a large untapped market for very low-cost vibration sensors for shutting off malfunctioning air-conditioning compressors to minimize the damage to equipment that is covered by manufacturers warranties. A break-through in vibration-sensor cost is needed to tap this market. The results of the successful completion of this project will be applicable to many other untapped markets for vibration sensors such as condition-based maintenance.

FY1999 Phase 2 Award Winner

TOPIC: 8.13 Building and Fire Research

SUBTOPIC: 8.13.12T Advanced Fire Suppression and Novel Suppression Concepts

TITLE: A Solid-Solid Hybrid Gas Generator Fire Suppression System

NIST OU: 860

FIRM: Mainstream Engineering Corporation

Pines Industrial Center

200 Yellow Place

Rockledge, FL 32955

PRINCIPAL INVESTIGATOR: Lawrence R. Grzyll

407-631-3550

AWARD AMOUNT: $299,771

ABSTRACT:

This Phase 2 proposal addresses the advanced development and commercialization of a novel solid-solid hybrid gas generator fire suppression technology to replace the ozone depleting Halon 1301 for total flooding applications. Mainstream's solid-solid hybrid gas generator technology will result in the delivery of chemical extinguishing agents to the fire in addition to the inert gas agents. This technology has several advantages over state-of-the art gas generator fire suppression technology. First, the system will be significantly smaller and lighter than current gas generator systems because it results in chemical, in addition to physical, extinguishment of the fire. Second, the entire hybrid gas generator material is stored in a single storage vessel as a solid, compared to other hybrid systems which require a separate pressure storage vessel. Third, the hybrid gas generator material has acceptable atmospheric and toxicological properties, unlike other hybrid gas generator systems that use the agents HFC-227ea., HFC-236FA, or CF3I.

COMMERCIAL APPLICATIONS:

Successful completion of the Phase 2 effort will result in the final development and commercialization of Mainstream's hybrid gas generation fire suppression technology. The Phase 2 effort will show that this technology is superior to other existing technologies in terms of system size, system weight, fire suppression effectiveness, and cost. The technology also has no environmental or atmospheric concerns, making it the ideal future technology for total flood fire suppression.

FY1999 Phase 2 Award Winner

TOPIC: 8.14 Information Technology

SUBTOPIC: 8.14.1T Extending RBAC to Include Work Flow Properties

TITLE: Workflow Policy Server

NIST OU: 890

FIRM: Secure Computing Corporation

2675 Long Lake Road

Roseville, MN 55113

PRINCIPAL INVESTIGATOR: Charles Payne

612-628-1584

AWARD AMOUNT: $299,398

ABSTRACT:

Workflow management systems (WMS) may control access between hundreds of users and thousands of objects, so simplified policy management is critical. WMS developers recommend Role-Based Access Control (RBAC) since roles occur naturally in workflows; however, the typical RBAC model lacks the framework to express workflow policies adequately.

Traditionally, a WMS mediates accesses to objects in its workflows. As workflow technology grows in popularity, workflows eventually may control distributed objects such as managed by CORBA and COM/DCOM. Protections must be added to these objects to prevent users from circumventing the WMS and accessing the objects directly.

We propose the "Workflow Policy Server" (WPS) to address these challenges. The WPS simplifies workflow policy management with a powerful RBAC Model that has been extended with workflow concepts. In particular, the concept of a workflow task or 'step' has been added. Distributed objects are protected because the WPS can "push out" the access control policy for a specific stop when directed. The WPS translates the step's policy into the enforcement language of the target object manager.

COMMERCIAL APPLICATIONS:

Secure Computing provides a wide family of high security products, including firewalls, web filtering software and authentication servers. One of the primary focuses is to provide centralized management of security components throughout the enterprise. Specifying and enforcing work flow policies accurately and easily is critical to enforcing complex business policies at several different locations.

Secure Computing intends to incorporate the work flow technology developed under this program into its suite of network security products.



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Date created: February 15, 2002

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